... Synthesis of (2S, 3R, 4S)-3,4-Methanoproline and Analogues . ... It was necessary to add a solution of the acid chloride in ether to lithium aluminium hydride in ether at - 80 o C, as addition of the hydride to the acid chloride led to up to 30 % of an ester derived by reaction of the product alcohol with the acid chloride. ... Hydrochloric acid (1 ml, 1M, 1 mmole) was added to the water layer and this was extracted with ether (2 x 5 ml). ... 1R, 2S, 5S)-3-Azabicyclo[3.1.0]hexane-2-carboxylic acid. ...

46. Студенческий форум Физфака МГУ > Электромагнитная модель атома, Крушева